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Viser: Introduction to Organic Laboratory Techniques - A Small-Scale Approach, International Edition
Introduction to Organic Laboratory Techniques
A Small-Scale Approach, International Edition
Randall G. Engel
(2010)
Sprog: Engelsk
Blue Kingfisher
1.691,00 kr.
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Detaljer om varen
- 3. Udgave
- Paperback: 1024 sider
- Udgiver: Blue Kingfisher (Maj 2010)
- ISBN: 9780538733281
Featuring new experiments, a new essay, and new coverage of nanotechnology, this organic chemistry laboratory textbook offers a comprehensive treatment of laboratory techniques including small scale and some microscale methods that use standard-scale ("macroscale") glassware and equipment. The book is organized based on essays and topics of current interest and covers a large number of traditional organic reactions and syntheses, as well as experiments with a biological or health science focus. Seven introductory technique-based experiments, thirteen project-based experiments, and sections on green chemistry and biofuels spark students' interest and engage them in the learning process. Instructors may choose to offer Cengage Learning's optional Premium Website, which contains videos on basic organic laboratory techniques.
Introduction.WELCOME TO ORGANIC CHEMISTRY.Laboratory Safety. Organization of the Textbook. Advance Preparation. Budgeting Time. Purpose.
Part One: The Techniques.Technique
1: Laboratory Safety.Technique
2: The Laboratory Notebook, Calculations, and Laboratory Records.Technique
3: Laboratory Glassware: Care and Cleaning.Technique
4: How to Find Data for Compounds: Handbooks and Catalogs.Technique
5: Measurement of Volume and Weight.Technique
6: Heating and Cooling Methods.Technique
7: Reaction Methods.Technique
8: Filtration.Technique
9: Physical Constants of Solids: The Melting Point.Technique
10: Solubility.Technique
11: Crystallization: Purification of Solids.Technique
12: Extractions, Separations, and Drying Agents.Technique
13: Physical Constants of Liquids: The Boiling Point and Density.Technique
14: Simple Distillation.Technique
15: Fractional Distillation, Azeotropes.Technique
16: Vacuum Distillation, Manometers.Technique
17: Sublimation.Technique
18: Steam Distillation.Technique
19: Column Chromatography.Technique
20: Thin-Layer Chromatography.Technique
21: High-Performance Liquid Chromatography (HPLC).Technique
22: Gas Chromatography.Technique
23: Polarimetry.Technique
24: Refractometry.Technique
25: Infrared Spectroscopy.Technique
26: Nuclear Magnetic Resonance Spectroscopy (Proton NMR).Technique
27: Carbon-13 Nuclear Magnetic Resonance Spectroscopy.Technique
28: 6 Mass Spectrometry.Technique
29: Guide to the Chemical Literature.
Part Two: Introduction to Basic Laboratory Techniques.Experiment
1: Solubility.Experiment
2: Crystallization.Experiment
3: Extraction.Experiment
4: A Separation and Purification Scheme.Experiment 4A: Extractions with a Separatory Funnel.Experiment
5: Chromatography.Experiment 5A: Thin-Layer Chromatography.Experiment 5B: Selecting the Correct Solvent for Thin-Layer Chromatography.Experiment 5C: Monitoring a Reaction with Thin Layer Chromatography.Experiment 5D: Column Chromatography.Experiment
6: Simple and Fractional Distillation.Experiment
7: Infrared Spectroscopy and Boiling-Point Determination.Experiment
8: Acetylsalicylic Acid.Experiment
9: Acetaminophen.Experiment
10: TLC Analysis of Analgesic Drugs.Experiment
11: Isolation of Caffeine.Experiment 11A: Extraction of Caffeine from Tea.Experiment 11B: Isolation of Caffeine from a Tea Bag.Experiment
12: Isopentyl Acetate (Banana Oil).Experiment
13: Isolation of Eugenol from Cloves.Experiment
14: Spearmint and Caraway Oil: (+)- and (-)-Carvones.Experiment
15: Isolation of Chlorophyll and Carotenoid Pigments from Spinach.Experiment
16: Ethanol from Sucrose.
Part Three: Introduction to Molecular Modeling.Experiment
17: An Introduction to Molecular Modeling.Experiment 17A: The Conformations of n-Butane: Local Minima.Experiment 17B: Cyclohexane Chair and Boat Conformations.Experiment 17C: Substituted Cyclohexane Rings (Critical Thinking Exercise).Experiment 17D: cis- and trans-2-Butene.Experiment
18: Computational Chemistry.Experiment 18A: Heats of Formation: Isomerism, Tautomerism, and Regioselectivity.Experiment 18B: Heats of Reaction: SN1 Reaction Rates.Experiment 18C: Density-Electrostatic Potential Maps: Acidities of Carboxylic Acids.Experiment 18D: Density-Electrostatic Potential Maps: Carbocations.Experiment 18E: Density-LUMO Maps: Reactivities of Carbonyl Groups.
Part Four: Preparations and Reactions of Organic Compounds.Experiment
19: Reactivities of Some Alkyl Halides.Experiment
20: Nucleophilic Substitution Reactions: Competing Nucleophiles.Experiment 20A: Competitive Nucleophiles with 1-Butanol or 2-Butanol.Experiment 20B: Competitive Nucleophiles with 2-Methyl-2-Propanol.Experiment 20C: Analysis.Experiment
21: Synthesis of n-Butyl Bromide and t-Pentyl Chloride.Experiment 21A: n-Butyl Bromide.Experiment 21B: t-Pentyl Chloride.Experiment
22: 4-Methylcyclohexene.Experiment
23: Methyl Stearate from Methyl Oleate.Experiment
24: Gas-Chromatographic Analysis of Gas
Part One: The Techniques.Technique
1: Laboratory Safety.Technique
2: The Laboratory Notebook, Calculations, and Laboratory Records.Technique
3: Laboratory Glassware: Care and Cleaning.Technique
4: How to Find Data for Compounds: Handbooks and Catalogs.Technique
5: Measurement of Volume and Weight.Technique
6: Heating and Cooling Methods.Technique
7: Reaction Methods.Technique
8: Filtration.Technique
9: Physical Constants of Solids: The Melting Point.Technique
10: Solubility.Technique
11: Crystallization: Purification of Solids.Technique
12: Extractions, Separations, and Drying Agents.Technique
13: Physical Constants of Liquids: The Boiling Point and Density.Technique
14: Simple Distillation.Technique
15: Fractional Distillation, Azeotropes.Technique
16: Vacuum Distillation, Manometers.Technique
17: Sublimation.Technique
18: Steam Distillation.Technique
19: Column Chromatography.Technique
20: Thin-Layer Chromatography.Technique
21: High-Performance Liquid Chromatography (HPLC).Technique
22: Gas Chromatography.Technique
23: Polarimetry.Technique
24: Refractometry.Technique
25: Infrared Spectroscopy.Technique
26: Nuclear Magnetic Resonance Spectroscopy (Proton NMR).Technique
27: Carbon-13 Nuclear Magnetic Resonance Spectroscopy.Technique
28: 6 Mass Spectrometry.Technique
29: Guide to the Chemical Literature.
Part Two: Introduction to Basic Laboratory Techniques.Experiment
1: Solubility.Experiment
2: Crystallization.Experiment
3: Extraction.Experiment
4: A Separation and Purification Scheme.Experiment 4A: Extractions with a Separatory Funnel.Experiment
5: Chromatography.Experiment 5A: Thin-Layer Chromatography.Experiment 5B: Selecting the Correct Solvent for Thin-Layer Chromatography.Experiment 5C: Monitoring a Reaction with Thin Layer Chromatography.Experiment 5D: Column Chromatography.Experiment
6: Simple and Fractional Distillation.Experiment
7: Infrared Spectroscopy and Boiling-Point Determination.Experiment
8: Acetylsalicylic Acid.Experiment
9: Acetaminophen.Experiment
10: TLC Analysis of Analgesic Drugs.Experiment
11: Isolation of Caffeine.Experiment 11A: Extraction of Caffeine from Tea.Experiment 11B: Isolation of Caffeine from a Tea Bag.Experiment
12: Isopentyl Acetate (Banana Oil).Experiment
13: Isolation of Eugenol from Cloves.Experiment
14: Spearmint and Caraway Oil: (+)- and (-)-Carvones.Experiment
15: Isolation of Chlorophyll and Carotenoid Pigments from Spinach.Experiment
16: Ethanol from Sucrose.
Part Three: Introduction to Molecular Modeling.Experiment
17: An Introduction to Molecular Modeling.Experiment 17A: The Conformations of n-Butane: Local Minima.Experiment 17B: Cyclohexane Chair and Boat Conformations.Experiment 17C: Substituted Cyclohexane Rings (Critical Thinking Exercise).Experiment 17D: cis- and trans-2-Butene.Experiment
18: Computational Chemistry.Experiment 18A: Heats of Formation: Isomerism, Tautomerism, and Regioselectivity.Experiment 18B: Heats of Reaction: SN1 Reaction Rates.Experiment 18C: Density-Electrostatic Potential Maps: Acidities of Carboxylic Acids.Experiment 18D: Density-Electrostatic Potential Maps: Carbocations.Experiment 18E: Density-LUMO Maps: Reactivities of Carbonyl Groups.
Part Four: Preparations and Reactions of Organic Compounds.Experiment
19: Reactivities of Some Alkyl Halides.Experiment
20: Nucleophilic Substitution Reactions: Competing Nucleophiles.Experiment 20A: Competitive Nucleophiles with 1-Butanol or 2-Butanol.Experiment 20B: Competitive Nucleophiles with 2-Methyl-2-Propanol.Experiment 20C: Analysis.Experiment
21: Synthesis of n-Butyl Bromide and t-Pentyl Chloride.Experiment 21A: n-Butyl Bromide.Experiment 21B: t-Pentyl Chloride.Experiment
22: 4-Methylcyclohexene.Experiment
23: Methyl Stearate from Methyl Oleate.Experiment
24: Gas-Chromatographic Analysis of Gas
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