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Viser: Introduction to Organic Laboratory Techniques - A Small-Scale Approach, International Edition
Introduction to Organic Laboratory Techniques
A Small-Scale Approach, International Edition
Randall G. Engel
(2010)
Sprog: Engelsk
om ca. 15 hverdage
Detaljer om varen
- 3. Udgave
- Paperback: 1024 sider
- Udgiver: Blue Kingfisher (Maj 2010)
- ISBN: 9780538733281
Part One: The Techniques.Technique
1: Laboratory Safety.Technique
2: The Laboratory Notebook, Calculations, and Laboratory Records.Technique
3: Laboratory Glassware: Care and Cleaning.Technique
4: How to Find Data for Compounds: Handbooks and Catalogs.Technique
5: Measurement of Volume and Weight.Technique
6: Heating and Cooling Methods.Technique
7: Reaction Methods.Technique
8: Filtration.Technique
9: Physical Constants of Solids: The Melting Point.Technique
10: Solubility.Technique
11: Crystallization: Purification of Solids.Technique
12: Extractions, Separations, and Drying Agents.Technique
13: Physical Constants of Liquids: The Boiling Point and Density.Technique
14: Simple Distillation.Technique
15: Fractional Distillation, Azeotropes.Technique
16: Vacuum Distillation, Manometers.Technique
17: Sublimation.Technique
18: Steam Distillation.Technique
19: Column Chromatography.Technique
20: Thin-Layer Chromatography.Technique
21: High-Performance Liquid Chromatography (HPLC).Technique
22: Gas Chromatography.Technique
23: Polarimetry.Technique
24: Refractometry.Technique
25: Infrared Spectroscopy.Technique
26: Nuclear Magnetic Resonance Spectroscopy (Proton NMR).Technique
27: Carbon-13 Nuclear Magnetic Resonance Spectroscopy.Technique
28: 6 Mass Spectrometry.Technique
29: Guide to the Chemical Literature.
Part Two: Introduction to Basic Laboratory Techniques.Experiment
1: Solubility.Experiment
2: Crystallization.Experiment
3: Extraction.Experiment
4: A Separation and Purification Scheme.Experiment 4A: Extractions with a Separatory Funnel.Experiment
5: Chromatography.Experiment 5A: Thin-Layer Chromatography.Experiment 5B: Selecting the Correct Solvent for Thin-Layer Chromatography.Experiment 5C: Monitoring a Reaction with Thin Layer Chromatography.Experiment 5D: Column Chromatography.Experiment
6: Simple and Fractional Distillation.Experiment
7: Infrared Spectroscopy and Boiling-Point Determination.Experiment
8: Acetylsalicylic Acid.Experiment
9: Acetaminophen.Experiment
10: TLC Analysis of Analgesic Drugs.Experiment
11: Isolation of Caffeine.Experiment 11A: Extraction of Caffeine from Tea.Experiment 11B: Isolation of Caffeine from a Tea Bag.Experiment
12: Isopentyl Acetate (Banana Oil).Experiment
13: Isolation of Eugenol from Cloves.Experiment
14: Spearmint and Caraway Oil: (+)- and (-)-Carvones.Experiment
15: Isolation of Chlorophyll and Carotenoid Pigments from Spinach.Experiment
16: Ethanol from Sucrose.
Part Three: Introduction to Molecular Modeling.Experiment
17: An Introduction to Molecular Modeling.Experiment 17A: The Conformations of n-Butane: Local Minima.Experiment 17B: Cyclohexane Chair and Boat Conformations.Experiment 17C: Substituted Cyclohexane Rings (Critical Thinking Exercise).Experiment 17D: cis- and trans-2-Butene.Experiment
18: Computational Chemistry.Experiment 18A: Heats of Formation: Isomerism, Tautomerism, and Regioselectivity.Experiment 18B: Heats of Reaction: SN1 Reaction Rates.Experiment 18C: Density-Electrostatic Potential Maps: Acidities of Carboxylic Acids.Experiment 18D: Density-Electrostatic Potential Maps: Carbocations.Experiment 18E: Density-LUMO Maps: Reactivities of Carbonyl Groups.
Part Four: Preparations and Reactions of Organic Compounds.Experiment
19: Reactivities of Some Alkyl Halides.Experiment
20: Nucleophilic Substitution Reactions: Competing Nucleophiles.Experiment 20A: Competitive Nucleophiles with 1-Butanol or 2-Butanol.Experiment 20B: Competitive Nucleophiles with 2-Methyl-2-Propanol.Experiment 20C: Analysis.Experiment
21: Synthesis of n-Butyl Bromide and t-Pentyl Chloride.Experiment 21A: n-Butyl Bromide.Experiment 21B: t-Pentyl Chloride.Experiment
22: 4-Methylcyclohexene.Experiment
23: Methyl Stearate from Methyl Oleate.Experiment
24: Gas-Chromatographic Analysis of Gas