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Viser: Experimental Electrochemistry
Experimental Electrochemistry
A Laboratory Textbook
Rudolf Holze
(2019)
Sprog: Engelsk
John Wiley & Sons, Limited
522,00 kr.
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Experimental Electrochemistry Vital Source e-bog
Rudolf Holze
(2019)
John Wiley & Sons
477,00 kr.
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Detaljer om varen
- 2. Udgave
- Paperback: 288 sider
- Udgiver: John Wiley & Sons, Limited (Oktober 2019)
- ISBN: 9783527335244
Showing how to apply the theoretical knowledge in practice, the one and only compilation of electrochemical experiments on the market now in a new edition.
Maintaining its didactic approach, this successful textbook provides clear and easy-to-follow instructions for carrying out the experiments, illustrating the most important principles and applications in modern electrochemistry, while pointing out the potential dangers and risks involved.
This second edition contains 84 experiments, many of which cover electrochemical energy conversion and storage as well as electrochemical equilibrium.
Maintaining its didactic approach, this successful textbook provides clear and easy-to-follow instructions for carrying out the experiments, illustrating the most important principles and applications in modern electrochemistry, while pointing out the potential dangers and risks involved.
This second edition contains 84 experiments, many of which cover electrochemical energy conversion and storage as well as electrochemical equilibrium.
Preface to the Second Edition ix Preface to the First Edition xi Foreword to the Second Edition xv Symbols and Acronyms xvii 1 Introduction: An Overview of Practical Electrochemistry 1 Practical Hints 2 Electrodes 3 Measuring Instruments 6 Electrochemical Cells 7 Data Recording 9 2 Electrochemistry in Equilibrium 11 Experiment
2.1: The Electrochemical Series 11 Experiment
2.2: Standard Electrode Potentials and the Mean Activity Coefficient 15 Experiment
2.3: pH Measurements and Potentiometrically Indicated Titrations 20 Experiment
2.4: Redox Titrations (Cerimetry) 25 Experiment
2.5: Differential Potentiometric Titration 27 Experiment
2.6: Potentiometric Measurement of the Kinetics of the Oxidation of Oxalic Acid 30 Experiment
2.7: Polarization and Decomposition Voltage 34 Experiment
2.8: A Simple Relative Hydrogen Electrode 39 3 Electrochemistry with Flowing Current 43 Experiment
3.1: Ion Movement in an Electric Field 44 Experiment
3.2: Paper Electrophoresis 46 Experiment
3.3: Charge Transport in Electrolyte Solution 47 Experiment
3.4: Conductance Titration 51 Experiment
3.5: Chemical Constitution and Electrolytic Conductance 54 Experiment
3.6: Faraday''s Law 56 Experiment
3.7: Kinetics of Ester Saponification 58 Experiment
3.8: Movement of Ions and Hittorf Transport Number 62 Experiment
3.9: Polarographic Investigation of the Electroreduction of Formaldehyde 68 Experiment
3.10: Galvanostatic Measurement of Stationary Current-Potential Curves 72 Experiment
3.11: Cyclic Voltammetry 75 Experiment
3.12: Slow Scan Cyclic Voltammetry 82 Experiment
3.13: Kinetic Investigations with Cyclic Voltammetry 86 Experiment
3.14: Numerical Simulation of Cyclic Voltammograms 90 Experiment
3.15: Cyclic Voltammetry with Microelectrodes 92 Experiment
3.16: Cyclic Voltammetry of Organic Molecules 96 Experiment
3.17: Cyclic Voltammetry in Nonaqueous Solutions 102 Experiment
3.18: Cyclic Voltammetry with Sequential Electrode Processes 104 Experiment
3.19: Cyclic Voltammetry of Aromatic Hydrocarbons 107 Experiment
3.20: Cyclic Voltammetry of Aniline and Polyaniline 110 Experiment
3.21: Galvanostatic Step Measurements 115 Experiment
3.22: Cyclic Voltammetry of a Supercapacitor Electrode 118 Experiment
3.23: Chronoamperometry 121 Experiment
3.24: Chronocoulometry 122 Experiment
3.25: Rotating Disk Electrode 124 Experiment
3.26: Rotating Ring-Disk Electrode 130 Experiment
3.27: Measurement of Electrode Impedances 133 Experiment
3.28: Corrosion Cells 136 Experiment
3.29: Aeration Cell 138 Experiment
3.30: Concentration Cell 139 Experiment
3.31: Salt Water Drop Experiment According to Evans 141 Experiment
3.32: Passivation and Activation of an Iron Surface 142 Experiment
3.33: Cyclic Voltammetry with Corroding Electrodes 143 Experiment
3.34: Tafel Plot of a Corroding Electrode 145 Experiment
3.35: Impedance of a Corroding Electrode 148 Experiment
3.36: Linear Polarization Resistance of a Corroding Electrode 150 Experiment
3.37: Oscillating Reactions 152 4 Analytical Electrochemistry 155 Experiment
4.1: Ion-Sensitive Electrode 156 Experiment
4.2: Potentiometrically Indicated Titrations 158 Experiment
4.3: Bipotentiometrically Indicated Titration 163 Experiment
4.4: Conductometrically Indicated Titration 165 Experiment
4.5: Electrogravimetry 167 Experiment
4.6: Coulometric Titration 170 Experiment
4.7: Amperometry 172 Experiment
4.8: Polarography (Fundamentals) 178 Experiment
4.9: Polarography (Advanced Methods) 182 Experiment
4.10: Anodic Stripping Voltammetry 183 Experiment
4.11: Abrasive Stripping Voltammetry 186 Experiment
4.12: Polarographic Analysis of Anions 189 Experiment
4.13: Tensammetry 191 5 Nontraditional Electrochemistry 197 Experiment
5.1: UV-Vis Spectroscopy 197 Experiment
5.2: Surface-Enhanced Raman Spectroscopy 200 Experiment
5.3: Surface-Enhanced Raman Spectroscopy of a Self-Assembled Monolayer 203 Experiment
5.4: Infrared Spectroelectrochemistry 205 Experiment
5.5: Electrochromism 207 Experiment
5.6: Raman Spectroscopic Monitoring of Charge/Discharge of an Intrinsically Conducting Polyaniline Supercapacitor Electrode Material 209 6 Electrochemical Energy Conversion and Storage 211 Experiment
6.1: Lead-Acid Accumulator 211 Experiment
6.2: Discharge Behavior of Nickel-Cadmium Accumulators 216 Experiment
6.3: Performance Data of a Fuel Cell 218 Experiment
6.4: Charging Supercapacitors 221 Experiment
6.5: Discharging Supercapacitors 224 Experiment
6.6: Zinc-Air Cell 227 Experiment
6.7: Lithium-Ion Battery 228 Experiment
6.8: Low-Temperature Discharge Behavior of Nickel-Cadmium Accumulators 230 Experiment
6.9: Discharge Behavior of Nickel-Cadmium Accumulators at Constant Load 233 Experiment
6.10: Impedance of a Button Cell 234 Experiment
6.11: Potentiostatic Polarization Curves 236 Experiment
6.12: Galvanostatic Polarization Curves 237 7 Electrochemical Production 241 Experiment
7.1: Cementation Reaction 241 Experiment
7.2: Galvanic Copper Deposition 242 Experiment
7.3: Electrochemical Oxidation of Aluminum 244 Experiment
7.4: Kolbe Electrolysis of Acetic Acid 245 Experiment
7.5: Electrolysis of Acetyl Acetone 247 Experiment
7.6: Anodic Oxidation of Malonic Acid Diethylester 250 Experiment
7.7: Indirect Anodic Dimerization of Acetoacetic Ester (3-Oxo-Butyric Acid Ethyl Ester) 251 Experiment
7.8: Electrochemical Bromination of Acetone 253 Experiment
7.9: Electrochemical Iodination of Ethanol 255 Experiment
7.10: Electrochemical Production of Potassium Peroxodisulfate 257 Experiment
7.11: Yield of Chlor-Alkali Electrolysis According to the Diaphragm Process 258 Appendix 261 Index 263
2.1: The Electrochemical Series 11 Experiment
2.2: Standard Electrode Potentials and the Mean Activity Coefficient 15 Experiment
2.3: pH Measurements and Potentiometrically Indicated Titrations 20 Experiment
2.4: Redox Titrations (Cerimetry) 25 Experiment
2.5: Differential Potentiometric Titration 27 Experiment
2.6: Potentiometric Measurement of the Kinetics of the Oxidation of Oxalic Acid 30 Experiment
2.7: Polarization and Decomposition Voltage 34 Experiment
2.8: A Simple Relative Hydrogen Electrode 39 3 Electrochemistry with Flowing Current 43 Experiment
3.1: Ion Movement in an Electric Field 44 Experiment
3.2: Paper Electrophoresis 46 Experiment
3.3: Charge Transport in Electrolyte Solution 47 Experiment
3.4: Conductance Titration 51 Experiment
3.5: Chemical Constitution and Electrolytic Conductance 54 Experiment
3.6: Faraday''s Law 56 Experiment
3.7: Kinetics of Ester Saponification 58 Experiment
3.8: Movement of Ions and Hittorf Transport Number 62 Experiment
3.9: Polarographic Investigation of the Electroreduction of Formaldehyde 68 Experiment
3.10: Galvanostatic Measurement of Stationary Current-Potential Curves 72 Experiment
3.11: Cyclic Voltammetry 75 Experiment
3.12: Slow Scan Cyclic Voltammetry 82 Experiment
3.13: Kinetic Investigations with Cyclic Voltammetry 86 Experiment
3.14: Numerical Simulation of Cyclic Voltammograms 90 Experiment
3.15: Cyclic Voltammetry with Microelectrodes 92 Experiment
3.16: Cyclic Voltammetry of Organic Molecules 96 Experiment
3.17: Cyclic Voltammetry in Nonaqueous Solutions 102 Experiment
3.18: Cyclic Voltammetry with Sequential Electrode Processes 104 Experiment
3.19: Cyclic Voltammetry of Aromatic Hydrocarbons 107 Experiment
3.20: Cyclic Voltammetry of Aniline and Polyaniline 110 Experiment
3.21: Galvanostatic Step Measurements 115 Experiment
3.22: Cyclic Voltammetry of a Supercapacitor Electrode 118 Experiment
3.23: Chronoamperometry 121 Experiment
3.24: Chronocoulometry 122 Experiment
3.25: Rotating Disk Electrode 124 Experiment
3.26: Rotating Ring-Disk Electrode 130 Experiment
3.27: Measurement of Electrode Impedances 133 Experiment
3.28: Corrosion Cells 136 Experiment
3.29: Aeration Cell 138 Experiment
3.30: Concentration Cell 139 Experiment
3.31: Salt Water Drop Experiment According to Evans 141 Experiment
3.32: Passivation and Activation of an Iron Surface 142 Experiment
3.33: Cyclic Voltammetry with Corroding Electrodes 143 Experiment
3.34: Tafel Plot of a Corroding Electrode 145 Experiment
3.35: Impedance of a Corroding Electrode 148 Experiment
3.36: Linear Polarization Resistance of a Corroding Electrode 150 Experiment
3.37: Oscillating Reactions 152 4 Analytical Electrochemistry 155 Experiment
4.1: Ion-Sensitive Electrode 156 Experiment
4.2: Potentiometrically Indicated Titrations 158 Experiment
4.3: Bipotentiometrically Indicated Titration 163 Experiment
4.4: Conductometrically Indicated Titration 165 Experiment
4.5: Electrogravimetry 167 Experiment
4.6: Coulometric Titration 170 Experiment
4.7: Amperometry 172 Experiment
4.8: Polarography (Fundamentals) 178 Experiment
4.9: Polarography (Advanced Methods) 182 Experiment
4.10: Anodic Stripping Voltammetry 183 Experiment
4.11: Abrasive Stripping Voltammetry 186 Experiment
4.12: Polarographic Analysis of Anions 189 Experiment
4.13: Tensammetry 191 5 Nontraditional Electrochemistry 197 Experiment
5.1: UV-Vis Spectroscopy 197 Experiment
5.2: Surface-Enhanced Raman Spectroscopy 200 Experiment
5.3: Surface-Enhanced Raman Spectroscopy of a Self-Assembled Monolayer 203 Experiment
5.4: Infrared Spectroelectrochemistry 205 Experiment
5.5: Electrochromism 207 Experiment
5.6: Raman Spectroscopic Monitoring of Charge/Discharge of an Intrinsically Conducting Polyaniline Supercapacitor Electrode Material 209 6 Electrochemical Energy Conversion and Storage 211 Experiment
6.1: Lead-Acid Accumulator 211 Experiment
6.2: Discharge Behavior of Nickel-Cadmium Accumulators 216 Experiment
6.3: Performance Data of a Fuel Cell 218 Experiment
6.4: Charging Supercapacitors 221 Experiment
6.5: Discharging Supercapacitors 224 Experiment
6.6: Zinc-Air Cell 227 Experiment
6.7: Lithium-Ion Battery 228 Experiment
6.8: Low-Temperature Discharge Behavior of Nickel-Cadmium Accumulators 230 Experiment
6.9: Discharge Behavior of Nickel-Cadmium Accumulators at Constant Load 233 Experiment
6.10: Impedance of a Button Cell 234 Experiment
6.11: Potentiostatic Polarization Curves 236 Experiment
6.12: Galvanostatic Polarization Curves 237 7 Electrochemical Production 241 Experiment
7.1: Cementation Reaction 241 Experiment
7.2: Galvanic Copper Deposition 242 Experiment
7.3: Electrochemical Oxidation of Aluminum 244 Experiment
7.4: Kolbe Electrolysis of Acetic Acid 245 Experiment
7.5: Electrolysis of Acetyl Acetone 247 Experiment
7.6: Anodic Oxidation of Malonic Acid Diethylester 250 Experiment
7.7: Indirect Anodic Dimerization of Acetoacetic Ester (3-Oxo-Butyric Acid Ethyl Ester) 251 Experiment
7.8: Electrochemical Bromination of Acetone 253 Experiment
7.9: Electrochemical Iodination of Ethanol 255 Experiment
7.10: Electrochemical Production of Potassium Peroxodisulfate 257 Experiment
7.11: Yield of Chlor-Alkali Electrolysis According to the Diaphragm Process 258 Appendix 261 Index 263
Detaljer om varen
- 2. Udgave
- Vital Source searchable e-book (Reflowable pages)
- Udgiver: John Wiley & Sons (Oktober 2019)
- ISBN: 9783527676293
Showing how to apply the theoretical knowledge in practice, the one and only compilation of electrochemical experiments on the market now in a new edition.
Maintaining its didactic approach, this successful textbook provides clear and easy-to-follow instructions for carrying out the experiments, illustrating the most important principles and applications in modern electrochemistry, while pointing out the potential dangers and risks involved.
This second edition contains 84 experiments, many of which cover electrochemical energy conversion and storage as well as electrochemical equilibrium.
Maintaining its didactic approach, this successful textbook provides clear and easy-to-follow instructions for carrying out the experiments, illustrating the most important principles and applications in modern electrochemistry, while pointing out the potential dangers and risks involved.
This second edition contains 84 experiments, many of which cover electrochemical energy conversion and storage as well as electrochemical equilibrium.
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